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The purification of organic compounds is a tedious, yet vital, part of synthetic organic chemistry. Successful organic synthesis requires very pure starting materials to avoid complications from impurities. When possible and practical, solids are purified via recrystallization or sublimation and liquids via distillation. In this experiment, students will purify crude acetanilide via ...

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DISTILLATION : PURIFICATION OF A MIXTURE OF MISCIBLE LIQUIDS EXPERIMENTAL TECHNIQUES REQUIRED Fractional distillation (T 10), greasing glass joints (T 11), gas chromatography (T 13) OTHER DOCUMENTS Experimental procedure, report template, gas chromatography traces INTRODUCTION Distillation is used separate miscible liquids based on differences ...

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CPI THF purification THF/water azeotrope n-Pentane Speciality chemicals Purification of 1,1,1,2-tetrafluoroethane (refrigerant) ... Separation of acetic acid and water by conventional distillation requires a very tall column, containing 70 to 80 trays. Preferably, the acid dehydration column in the sol- vent recovery unit can be operated as an azeotropic distillation column. As an example, let ...

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